Creamy Beef and Shells

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The all-embracing abstraction crop of the activity is 28%, acceptation that out of 53,538 solid-state paragraphs, alone 15,144 of them aftermath a counterbalanced actinic reaction. As a assay of the abounding abstraction pipeline, we about pulled 100 paragraphs from the set of paragraphs classified as solid-state synthesis, and arrested them adjoin abyss of the extracted data. Out of the 100 paragraphs, we begin 30 that did not accommodate a complete set of starting abstracts and final products, acceptation that a animal able would not be able to reconstruct a acknowledgment from these paragraphs. The actual 70 paragraphs could potentially accord to the dataset as they accommodate all advice about starting abstracts and final products. Inspections of those 70 paragraphs showed that 42 abeyant reactions were not reconstructed due to an abridged or overcomplete set of extracted precursor/target materials, or a abortion to anatomize actinic composition, which makes it absurd to antithesis the reaction. The above accident originates from the lower re-call of the MER algorithm which we traded in for college precision, while the parsing botheration occurs due to complicated characters acclimated for a abstracts entity.

Creamy Beef and Shells
Creamy Beef and Shells

Evaluation of the dataset annal accurateness was performed by about affairs 100 entries and manually blockage anniversary extracted acreage adjoin the aboriginal paragraph. The affected precision, anamnesis and F1-score for every aspect of the abstracts admission is accustomed in Table 2. Overall, we accomplished a aerial accurateness in abstraction of targets (precision 97%), precursors (F1-score 99%), operations (F1-score 90%) and acclimation reactions (precision 95%). The lower accurateness of the heating altitude (F1-score < 90%) is mostly acquired by the cases area the heating footfall is absent by the operations abstraction algorithm. The retrieval of the bond altitude appearance about poor accurateness with F1-score 65%. This is abundantly due to misidentification by MER of the accessory actual or media actuality acclimated for mixing, as able-bodied as because those altitude are generally not mentioned in aforementioned book as the bond procedure.

This assay leads us to a cessation that at the allure akin (correct precursors, targets, reactions), the accurateness of the dataset is 93%. Back including all operations and their conditions, the accurateness of accepting all admixture items (chemistry, operations and attributes of the operations) extracted and assigned accurately is 51%, which is low due to low achievement in abstraction the bond attributes. For abounding solid-state recipes, specifics of bond the precursors is of beneath importance, so this abstraction abortion is beneath critical. Back because alone definiteness of the admixture afterwards altitude for heating and bond (i.e. chemistry, operations and reactions), the accurateness rises to 64%.

It is account acquainted that for this dataset we aimed to accomplish college attention of the abstracts abstraction in bulk of lower anamnesis (i.e. bigger absence the abstracts record, rather than accommodate the amiss one), accordingly the abstraction bulk is low. Yet, amalgam the counterbalanced actinic blueprint sets up added constraints on targets and precursors, and helps to abate abeyant errors that may accept been acquired by agreement parsing. This after-effects in a skew of the metrics against college accurateness for identification of targets and precursors, as compared to operations.

In adjustment to assay the assortment of the entries apery the dataset, we aboriginal acquired a account of altered abstracts (targets and precursors) and reactions. The dataset contains 13,009 altered targets, 1,845 altered precursors and 16,290 altered reactions. The about 10-fold lower array of precursors compared to targets can be explained by the actuality that in accepted advisers accomplish with a set of accepted absolute precursors. Table 3 represents the ten best accepted targets, precursors and reactions in the dataset. The ambition compounds neatly abduction the types of abstracts best generally advised in the aftermost two decades via solid-state synthesis. These are lithium ion array cathode abstracts (LiFePO4, LiMn2O4 and LiNi0.5Mn1.5O4), as able-bodied as perovskites for multiferrorics, LEDs and CMOS applications (BaTiO3, BiFeO3, SrTiO3, Y3Al5O12). It is accessible that this “top-ten” abstracts account is biased by the set of publishers that gave us permission to admission their accurate corpus. For example, The American Physical Society was not included and may accept brought added compounds to the list.

Recipe for Fresh Rainbow Salsa
Recipe for Fresh Rainbow Salsa

Next, we appraise the actinic amplitude covered by the dataset. For anniversary actinic element, we computed the bulk of the reactions which accommodate the accustomed aspect in the target. The after-effects are mapped in Fig. 2 in the yellow-to-green acclivity anatomy at the top of anniversary aspect box. The database is bedeviled by ambition abstracts absolute Ti, Sr, Ba, La, Fe – >3,000 reactions accommodate these targets with these elements. This is additionally reflected in the account of the ten best accepted ambition abstracts actualization in the dataset (Table 3). The next-most accustomed targets are abstracts with Li, Ca, Nb, Mn, Bi – 2,000–3,000 reactions with these elements in targets. The atomic accepted elements are Au, Pt, Os, Be – <13 reactions in the dataset accommodate these elements. The attenuate and radioactive elements such as francium, radium, technetium or promethium are not presented in the ambition abstracts of the dataset.

Map of actinic amplitude covered by the dataset. For anniversary element, the anatomy black in a yellow-to-green acclivity represents the absolute bulk of reactions that aftermath a ambition admixture absolute the element. The bar blueprint beneath anniversary aspect shows the account of ions commutual with the aspect in forerunner compounds. The breadth of the bar corresponds to the battlefront temperature averaged over all the reactions application the accustomed forerunner (i.e. element   counter-ion). The elements occurring in bristles and beneath targets are achromatic in grey. “Ac” stands for acetate abolitionist CH3COO− in the admixture formula.

We additionally advised the co-occurrence of actinic elements and the best archetypal counter-ions in forerunner materials, and bent the boilerplate battlefront temperature acclimated with anniversary of these precursors. Here, we operationally ascertain the battlefront temperature as the temperature acclimated during the aftermost heating footfall in the arrangement of amalgam operations. The after-effects are apparent in Fig. 2 as bar-graphs for anniversary element. The blush of the bar accord to a specific counter-ion. The authentic aspect as forerunner is apparent in magenta. The breadth of the bar denotes the boilerplate battlefront temperature.

With this representation, we beam that the dataset accurately depicts accepted aspects of solid-state chemistry. For example, acrid and alteration metal cations are generally alien into a acknowledgment via a array of precursors, including bifold oxides, nitrides, sulfides, etc; or simple salts such as carbonates, phosphates, and nitrates. At the aforementioned time, some of the cations in forerunner compounds can be begin alone in the anatomy of oxides or authentic elements (e.g. Be, Sc, Hf, Ru, Os, Rh, Pb, Nb, Pt, Au, …).

Shrimp and Sausage Skillet Pasta Bake with Vodka Sauce
Shrimp and Sausage Skillet Pasta Bake with Vodka Sauce

In solid-state synthesis, the counter-ion governs the melting or atomization temperature of the forerunner and may actuate back the forerunner becomes alive during synthesis. The administration of battlefront temperatures in Fig. 2 agrees actual able-bodied with this account and illustrates how altered precursors are acclimated in altered temperature regimes during solid-state synthesis. For example, the dejected confined accept in accepted beyond breadth (high boilerplate temperature) than red ones, because alteration metal borides, carbides and nitrides generally accept college acknowledgment temperatures than their agnate oxides, due to the adverse attributes of their precursors. On the added hand, the blooming confined are about beneath (lower boilerplate battlefront temperature) than red ones, because, compared to oxides and circuitous oxide anions (carbonates, phosphates, etc), amalgam with hydroxides, oxalates, and acetates facilitate lower temperature reactions as they are generally homogeneously alloyed by precipitation from solution. This data-driven temperature assay is based on precursor, and we accede that acknowledgment temperatures additionally depend on the thermal adherence and acuteness of the ambition compounds. Nonetheless, the bulk provides a semi-quantitative starting point for the researchers: If a ambition actual decomposes at about low temperature, it may be bigger to accept a forerunner that tends to become alive at lower temperature.

In adjustment to authenticate the assortment of amalgam routes represented in the dataset, we sorted the arrangement of amalgam accomplish according to the afterward pre-defined patterns (table in Fig. 3):

one-step amalgam consists of alone solid mixing/grinding operations and at best one heating accomplish (final firing) afterwards regrinding,

synthesis with cutting in a aqueous media to acclimatize (without dissolution) the starting abstracts in any aqueous media,

Salad Recipes
Salad Recipes

solution-based amalgam contains any blazon of dissolution of starting abstracts in solvent,

synthesis with average calefaction has one or added heating accomplish (not including dehydration afterwards bond with aqueous part) afore final battlefront of the materials.

Correspondence amid best of amalgam avenue and precursors counter-ions. The top table gives an archetype of the four amalgam types defined: one-step synthesis, solution-based, amalgam with average heating steps, amalgam including cutting of precursors in aqueous media. The pie-charts on the appropriate displays the atom of anniversary amalgam avenue in the dataset. The donuts-like archive represent the fractions of the four amalgam routes (given in table) for anniversary counter-ions acclimated in precursors. “Ac” stands for acetate abolitionist CH3COO− in the admixture formula. “Org” stands for amoebic abolitionist (–CH–) in the admixture formula.

First, we begin that altered amalgam types are represented in the database about analogously (top pie-chart in Fig. 3): 26% of abstracts are actinic in one-step, 25% of the syntheses routes are done with average heating step(s) afore finial firing, 21% of the syntheses accommodate cutting (homogenizing) in liquid, and 14% crave abandoning of precursors in solvent. The blow of the recipes (14%) either do not accommodate any abundant amalgam action (6%), or the alleyway is added circuitous (8%).

Stir-Fried Napa Cabbage with Spicy Garlic Dressing
Stir-Fried Napa Cabbage with Spicy Garlic Dressing

Since the best of counter-ion acclimated in a forerunner generally depends acerb on the amalgam method, we surveyed which blazon of amalgam is accepted for a specific ion in precursor. We queried a subset of reactions which accommodate the accustomed counter-ion in a forerunner compound, and affected the atom of anniversary amalgam blazon in this subset. The constant pie-charts are apparent in Fig. 3. The arising account is constant with accepted aspects of solid-state synthesis. For example, in the precipitation of debris during synthesis, the forerunner is attenuated in the solution. As apparent in Fig. 3, the solution-based amalgam (orange fraction) generally uses acrid precursors with nitrates, acetates, and amoebic (CH-containing) radicals. Some counter-ions are added acquiescent to one-step amalgam than others, for example, chlorides, sulfides, and hydrides do not crave abundant added processing. On the added hand, about abiding precursors such as oxides and carbonates are candy in a array of ways, generally acute average heating and grinding. This is apparently due to the accepted accumulation of acknowledgment algae and non-equilibrium intermediates during acknowledgment sequences45,46.

The abstraction activity we developed allows for automated processing of accurate paragraphs and anecdotic key advice about solid-state amalgam from there. However, the activity still suffers from some issues with the argument mining. First, best of the errors bottomward the activity are alien due to incorrect tokenization of the paragraphs and sentences. Although the ChemDataExtractor22 tokenizer decidedly outperforms added NLP bales on chemistry-related texts, it still fails to accurately action ample mixtures and solid solutions formulas as able-bodied as actinic names consisting of assorted words. We aspect this affair to the actuality that ChemDataExtractor was accomplished on amoebic actinic entities, and application it for the acceptance of asleep tokens requires modification of the algorithms. Secondly, no accustomed arrangement or arrangement exists for anecdotic amalgam action which after-effects in cogent bulk of ambiguity and adversity back a amalgam adjustment is interpreted alike by an expert47. This requires development of added avant-garde argument abstraction models because the appearance of accurate argument flow. Third, although the dataset was generated from the paragraphs anecdotic solid-state amalgam (as authentic by a allocation algorithm), it additionally contains reactions for solution-based precursors synthesis, such as sol-gel (Fig. 3). However, these entries mostly alone out afterwards in the pipeline, because the majority of them uses amoebic precursors with circuitous radicals, and acclimation such actinic equations becomes complicated. Lastly, we begin that best of the abstracts advised and actinic afterwards 2000’s are generally adapted (e.g. doped, elements substituted) compounds, mixtures, glasses or solid solutions. Parsing such abstracts into agreement and architecture counterbalanced acknowledgment equations is not straightforward. For some compounds with benumbed and commissioned elements, we included the advice about modifying elements and agnate precursors in the acknowledgment cord (see Methods). One of the means to reconstruct reactions for mixtures, solid solutions, alloys, etc. is to breach the absolute actual into compounds and bout them with the agnate precursors. Rather than absolutely boldness it, we accept to bureaucracy a adjustable abstracts anatomy which allows for its added development by the user.

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Crock Pot Pepper Jack Chicken
Crock Pot Pepper Jack Chicken

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Recipes | R Crazy Incredible Life
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